HPTLC Silica gel 60 DIOL F₂₅₄s

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一般描述

Our NH2, CN and DIOL -modified silica sorbents are less polar then conventional silica phases, making them ideal for separating hydrophilic or charged substances. Our moderately polar cyano- and diol-modified silica plates can be used for both normal phase and reversed phase systems. An alternative to PEI cellulose, amino-modified NH2 plates provide weak basic ion exchange characteristics with special selectivity for charged compounds.
25 Glass plates 20 x 10 cm

分析说明

Specific surface area (according to BET; 5-Pt. measurement): 480 - 540 m?/g
Pore volume (N?-isotherm): 0.74 - 0.84 ml/g
d 50 (laser diffraction, size distribution): 5 - 7 ?m
Layer thickness: 150 - 200 ?m
Deviation of layer thickness per plate: ≤ 35 ?m
Chromatographic testings:
A) Steroidtest, straight phase
hRf-values
- hydrocortisone, straight phase:
4 - 8
- Reichstein S, straight phase: 11 - 18
- Methyltestosterone, straight phase: 27 - 36
B) Steroid test, reversed phase
- methyltestosterone, steroid test: 48 - 68
- Reichstein S, steroid test: 58 - 78
- hydrocortisone, steroid test: 68 - 88
Typical value determined on an activated plate (120°C, 15 min)
Eluent a) petroleum benzine 40-60°/acetone (80/20 v/v)
Eluent b) acetone/water (30/70 v/v)

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