半岛bd体育手机客户端 说明

应用

Screening kit for Miyaura borylation reaction. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets

Each kit contains 2 customizable screening sets that include the following components:

• 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
• 4 x 4 mL reaction vials with pre-weighed KOAc
• Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
• 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
• 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
• 4 stir bars for substrate stock solution vials.
• 1 internal standard.

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

特点和优势

• Designed and tested by synthetic chemists.
• Easily run 24-microscale reactions in parallel.
• 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
• Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

法律信息

KitAlysis is a trademark of sigma-aldrich Co. LLC

半岛bd体育手机客户端 性质

reaction suitability	reaction type: Buchwald-Hartwig Cross Coupling Reaction reaction type: Cross Couplings reaction type: Heck Reaction reaction type: Hiyama Coupling reaction type: Negishi Coupling reaction type: Sonogashira Coupling reaction type: Stille Coupling reaction type: Suzuki-Miyaura Coupling reagent type: catalyst core: palladium
官能团	phosphine

组份列表

组份可单独销售

货号	组份
764175	P(Cy3) Pd G3, 97%
791733	Potassium acetate, anhydrous, free-flowing, Redi-Dri?, ACS reagent, ≥99.0%
804274	XPhos Pd G4, 95%
804282	SPhos Pd G4
804290	RuPhos Pd G4
804975	DTBPF-Pd-G3
900349	cataCXium Pd G4
900522	Toluene, anhydrous, ZerO2?, 99.8%
900631	Ethylene glycol, anhydrous, ZerO2?, 99.8%
900634	N,N-Dimethylacetamide, anhydrous, ZerO2?, 99.8%
900636	Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2?, ≥99.9%
900639	1-Butanol, anhydrous, ZerO2?, 99.8%
900641	Methanol, anhydrous, ZerO2?, 99.8%
900644	Acetonitrile, anhydrous, ZerO2?, 99.8%
900690	N,N-Diisopropylethylamine, purified by redistillation, ZerO2?, 99.5%
221171	Pinacol, 98%
473294	Bis(pinacolato)diboron, 99%
754242	Tetrahydroxydiboron, 95%
B34656	Biphenyl, ReagentPlus?, 99.5%
Z118850	Spinbar?magnetic stirring fleas, red, L 10 mm, diam. 3 mm
Z742110	KitAlysis?24-well reaction block replacement film

安全信息

象形图
警示用语：	Danger
危险声明	H225 - H301 + H311 + H331 - H315 - H318 - H335 - H336 - H351 - H360D - H370 - H373 - H410
预防措施声明	P210 - P273 - P280 - P301 + P310 - P303 + P361 + P353 - P305 + P351 + P338
危险分类	Acute Tox. 3 Dermal - Acute Tox. 3 Inhalation - Acute Tox. 3 Oral - Aquatic Acute 1 - Aquatic Chronic 1 - Carc. 2 - Eye Dam. 1 - Flam. Liq. 2 - Repr. 1B - Skin Irrit. 2 - STOT RE 2 Oral - STOT SE 1
靶器官	Kidney
补充剂危害	EUH019
储存分类代码	3 - Flammable liquids
WGK	WGK 3
闪点(F)	1.4 °F
闪点(C)	-17 ℃