STA-FTIR 鑱旂敤鎶€鏈殑闈╂柊

閫稿嚭姘斾綋鍒嗘瀽鏄竴绉嶇敤鏉ュ垎鏋愭湁鏈恒€佹棤鏈虹被鍥轰綋鎴栨恫浣撴牱鍝佺殑鐑晥搴旓紝浠ュ強鐩稿簲鍖栧鎬ц川鍙樺寲鐨勭悊鎯冲伐鍏枫€侟/p>

鍏ㄦ柊鐨 Perseus STA 449F1/F3 鑱旂敤绯荤粺鏄 NETZSCH STA 449 F1/F3 Jupiter^?鍚屾鐑垎鏋愪华涓 Bruker ALPHA FT-IR 绾㈠鍏夎氨浠殑瀹岀編缁撳悎銆傚畠闈╁懡鎬х殑璁捐宸茬粡鎴愪负浜嗚仈鐢ㄦ妧鏈殑涓€涓柊鐨勯噷绋嬬銆侟/p>

璇ヨ仈鐢ㄧ郴缁熷叿鏈夐珮鎬ц兘锛岄珮鍏煎鎬э紝璁捐绱у噾鐨勭壒鐐癸紝閫傚悎浜庡悇绉嶄粠浜嬫棤鏈烘垨楂樺垎瀛愯仛鍚堢墿鍏夎氨鍒嗘瀽鐨勯珮鏍＄爺绌跺鍜屽伐涓氱爺鍙戦儴闂ㄣ€侟/p>

浠讳綍宸叉湁鐨 NETZSCH STA F1/F3 绯荤粺閮借兘鍗囩骇鑷 Persus-STA-FTIR 鑱旂敤绯荤粺銆侟/p>

楂樻€т环姣旂殑姘斾綋鍒嗘瀽鎶€鏈?/h4>

Persus-STA-FTIR 鑱旂敤绯荤粺鎬ц兘寮哄ぇ锛屼环鏍奸€備腑锛岃兘澶熻緝骞挎硾鍦拌鍚勭绫诲瀷鐨勫疄楠屽鎵€浣跨敤銆侟/p>

鏃犻渶娑叉爱

鑱旂敤绯荤粺鐨 FTIR 閮ㄥ垎閲囩敤 DTGS锛坉euterated triglycine sulphate锛屾皹鐢樻皑閰哥～閰哥洂锛夋娴嬪櫒锛屼笉鍐嶉渶瑕佷娇鐢ㄦ恫姘喎鍗淬€傝绯荤粺鐗瑰埆閫傚悎鍦ㄨ嚜鍔ㄨ繘鏍锋垨鑰呭疄楠屾椂闂磋緝闀跨殑鎯呭喌涓嬩娇鐢ㄣ€侟/p>

鏃犻渶鍗曠嫭鐨勬皵浣撲紶杈撶绾军/h4>

璇ヨ仈鐢ㄧ郴缁熶笉鍐嶉渶瑕佹皵浣撲紶杈撶绾裤€傚唴缃殑姘斾綋鍔犵儹鍗曞厓閫氳繃鍔犵儹绠＄洿鎺ヤ笌鐐変綋鐨勫嚭姘斿彛鐩歌繛銆傝繖绉嶈秴鐭殑姘旇矾璁捐淇濊瘉浜嗗揩閫熺殑鍝嶅簲锛岃兘澶熷湪鏈€澶х▼搴︿笂閬垮厤閫稿嚭姘斾綋鐨勫喎鍑濄€侟/p>

绱у噾鐨勮璁狘/h4>

Persus-STA-FTIR 鑱旂敤绯荤粺璁捐绱у噾锛屽叾 FTIR 閮ㄥ垎鐩存帴瀹夎浜 STA 鐨勪笂鏂癸紝鑰岄潪涓 STA 骞跺垪鏀剧疆銆傚嵆浣垮浜庣┖闂存湁闄愮殑瀹為獙瀹わ紝涔熶笉蹇呮媴蹇冧华鍣ㄦ憜鏀剧殑闂銆侟/p>

Perseus-STA 绯荤粺鍙互琚簲鐢ㄤ簬濡備笅鐮旂┒锛欬/p>

• 鍒嗚В

• 姘斿浐鍙嶅簲

• 缁勫垎鍒嗘瀽

• 鎸ュ彂锛屾皵浣撻噴鍑裹/p>

Perseus STA-FTIR - 鎶€鏈壒鎬э紙鎸佺画鏇存柊涓級

姘斾綋鍗曞厓闀垮害/瀹圭Н锛?0mm / 5.8ml锛堝唴閮ㄦ棤鍙嶅皠闀滐紝鍏夎矾绋冲畾锛堻/p> 妫€娴嬪櫒锛欴TGS 姘斾綋鍗曞厓鍔犵儹锛氭渶楂 200掳C锛岃蒋浠舵帶鍒迭/p> 绾㈠娉㈡暟鑼冨洿锛?000cm-1... 500cm-1 姘斾綋鍗曞厓鐨勭獥浣撴潗鏂欙細ZnSe 浼犺緭绠＄殑鍔犵儹锛氫袱绉嶆柟寮忓彲閫夛紙娓╁害鎺у埗锛涙亽瀹氬姛鐜囧姞鐑級

Perseus STA-FTIR - 杞欢鍔熻兘

鐑垎鏋愪华鍩烘湰杞欢 Proteus^?杞欢涓 FT-IR 鍩烘湰杞欢 OPUS 鍧囪繍琛屽湪 Windows^?骞冲彴涓嬨€備袱鑰呯浉浜掗泦鎴愶紝鍏卞悓鍗忎綔锛屾瀯鎴愪簡 Perseus STA F1/F3 鑱旂敤绯荤粺鐨勬祴閲忎笌鏁版嵁鍒嗘瀽杞欢绯荤粺銆傚浜庢鍦ㄨ繍琛岀殑娴嬮噺锛岃兘澶熶互娓╁害鎴栨椂闂磋氨鐨勫舰寮忔樉绀洪噰闆嗗埌鐨勫悇绉嶆暟鎹€侟/p>

Proteus^?杞欢鍖呭惈寮哄ぇ鐨勬祴閲忓拰鏁版嵁鍒嗘瀽鍔熻兘锛屽叿鏈夋瀬鍏跺弸鍠勭殑鐢ㄦ埛鐣岄潰锛屽寘鎷槗浜庣悊瑙ｇ殑鑿滃崟鎿嶄綔鍜岃嚜鍔ㄦ搷浣滄祦绋嬶紝骞朵笖閫傜敤浜庡悇绉嶅鏉傜殑鍒嗘瀽銆侾roteus^?杞欢鏃㈠彲瀹夎鍦ㄤ华鍣ㄧ殑鎺у埗鐢佃剳涓婅仈鏈哄伐浣滐紝涔熷彲瀹夎鍦ㄥ叾浠栫數鑴戜笂鑴辨満浣跨敤銆侟/p>

閮ㄥ垎鐗规€?

• 浣跨敤 NETZSCH Proteus^?杞欢杩涜鐑垎鏋愭暟鎹殑閲囬泦銆佸瓨鍌ㄤ笌鍒嗘瀽锛屼娇鐢 BrukerOptik OPUS 杞欢杩涜绾㈠鍏夎氨鏁版嵁鐨勯噰闆嗐€佸瓨鍌ㄤ笌鍒嗘瀽銆備袱鑰呬箣闂村彲杈惧埌瀹炴椂鍚屾銆侟/p>

• 浣跨敤 OPUS/CHROM 杞欢锛屽彲缁樺嚭 FTIR 涓 STA 娴嬭瘯鏇茬嚎鐩稿浜庢椂闂翠笌娓╁害鐨勪簩缁存垨涓夌淮鍥俱€侟/p>

• 浣跨敤 OPUS/SEARCH 鍔熻兘锛屽彲杩涜绾㈠璋卞浘鐨勬暟鎹簱鎼滅储銆侟/p>

• Proteus 杞欢鍙鍏 FTIR 鍥捐氨锛屼笌瀵瑰簲鐨 STA 鍥捐氨涓€璧疯繘琛屽垎鏋愶紝鏍囨敞鐗瑰緛娓╁害涓庡嘲闈㈢Н銆侟/p>

• Gram-Schmidt 鍥撅紝鍙繘琛屾俯搴︿笌宄伴潰绉绠楋紝鍙笌鐑垎鏋愭洸绾夸竴璧疯繘琛屽垎鏋愩€侟/p>

TGA-FT-IR 鑱氬悎鐗╂暟鎹簱

TGA-FT-IR 鑱氬悎鐗╂暟鎹簱鍖呭惈鐢 TGA-FT-IR 鑱旂敤鎶€鏈祴寰楃殑銆佹潵鑷 88 绉嶈仛鍚堢墿鐨勮秴杩 129 绉嶆皵鐩歌氨鍥撅紝浠庤繖浜 FT-IR 鍏夎氨鍥句腑鍙互鑾峰彇杩欎簺鑱氬悎鐗╁湪鍒嗚В鏈€澶ч€熺巼鐐癸紙DTG 宄版俯锛夌殑閫稿嚭姘斾綋鐨勭粍鍒嗕俊鎭€傝鏁版嵁搴撻€傜敤浜 NETZSCH-Bruker 鐑孩鑱旂敤浠櫒锛屽彲浠ラ泦鎴愬湪 OPUS 鍏夎氨妫€绱㈣蒋浠朵箣涓€侟/p>

濡傞渶鑾峰彇璇ユ暟鎹簱锛岃鑱旂郴鑰愰┌鍏徃鐩稿叧閿€鍞笌鎶€鏈湇鍔″伐绋嬪笀銆侟br class="Apple-interchange-newline"/>

Perseus STA-FTIR - 搴旂敤瀹炰緥

Perseus STA 449 F1/F3 鑱旂敤绯荤粺鍙簲鐢ㄤ簬涓嬪垪棰嗗煙锛欬/p>

• 鍒嗚В

• 姘?鍥哄弽搴擖/p>

• 缁勫垎鍒嗘瀽

• 钂稿彂锛屾尌鍙慄/p>

绉哥

绉哥鏄劚绮掑苟鏅掑共鐨勭帀绫崇锛屼篃鍖呮嫭涓€浜涚敤浜庢Θ娌瑰拰鍒朵綔绾ょ淮鐨勬鐗╃殑鍙跺瓙绛夈€傞櫎浜嗗啘涓氫笂鐨勫簲鐢ㄥ锛岀Ц绉嗕篃鏈夊彲鑳芥垚涓烘湭鏉ヨ兘婧愮殑閲嶈杞戒綋銆傛澶勶紝鎴戜滑灏 28.6 mg 鐨勭Ц绉嗙矇鏈湪 N2 姘旀皼涓嬩互 20 K/min 鐨勯€熺巼杩涜鍔犵儹锛屼互瀵瑰叾鐑涓鸿繘琛岃〃寰併€侟/p>

鐢 TGA 鏇茬嚎鍙锛屾牱鍝佸垎鍒湪 110掳C锛?98掳C 鍜 356掳C 锛圖TG 宄板€兼俯搴︼級鍑虹幇澶遍噸鍙伴樁銆傚湪 400掳C 浠ヤ笂锛屽垯鍑虹幇缂撴參鎸佺画鐨勫け閲嶈繃绋嬨€傚搴旂殑澶遍噸閲忎负锛氱脳闃舵 5%锛岀浉浜掗噸鍙犵殑绗簩銆佺涓夐樁娈靛垎鍒负 33.4% 涓 25.3%锛岀鍥涢樁娈 10.7%銆?40掳C 涓嬬殑娈嬩綑璐ㄩ噺涓 25.6%銆侟/p>

鐩稿簲鐨勭孩澶栬氨鍥炬樉绀猴紝TGA 绗楅樁娈靛け閲嶏紙110掳C锛夋槸鐢辨牱鍝佽劚姘村紩璧凤紝鑰 298掳C 涓 356掳C 鐨勫け閲嶅垯涓庢按锛孋O锛孋O2锛岀敳閰革紝涔欓吀鍜屼箼鐑风殑閲婃斁鏈夊叧銆傛澶栵紝鍦 534掳C闄勮繎杩樺嚭鐜颁簡鐢茬兎鐨勯噴鏀俱€傚湪NETZSCH Proteus^?杞欢涓紝鑳藉杞绘澗鍦板鍏ヤ笌 TGA 鍜 DTG 鏇茬嚎鐩稿搴旂殑 FTIR 鏇茬嚎銆侟/p>

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娣峰悎寤虹瓚鏉愭枡

鐭崇伆锛圕aCO3锛夈€佺啛鐭崇伆锛圕a(OH)2锛夈€佺煶鑻憋紙SiO2锛夊拰鐭宠啅锛堜簩姘村悎纭吀閽欙級浣滀负缁忓吀鐨勫缓绛戞潗鏂欒骞挎硾浣跨敤銆傚湪杩欎釜瀹為獙涓紝杩欎簺鐗╄川鐨勬贩鍚堢墿琚斁缃簬 Pt/Rh 鍧╁煔涓紝鍦ㄧ┖姘旀皵姘涗笅浠 20K/min 鐨勫崌娓╅€熺巼鍔犵儹鑷 1500鈩冦€侟br/>涓嬪浘鎵€绀轰负鏁翠釜鍔犵儹杩囩▼涓殑 TGA 涓 DSC鏇茬嚎銆俆GA 鏇茬嚎涓嚭鐜颁簡鑻ュ共涓け閲嶆楠わ紝鍏跺搴旂殑 DSC 宄板垎鍒槸鍦 150鈩冦€?53鈩冦€?79鈩 闄勮繎锛屾渶鍚庣殑澶遍噸宄板嚭鐜板湪 1300鈩 涓 1400鈩 涔嬮棿銆傚湪 DSC 鏇茬嚎涓婏紝杩樺嚭鐜颁簡鍑犱釜棰濆鐨勫皬宄帮細362鈩 鍑虹幇浜嗕竴涓皬鐨勬斁鐑嘲锛?76鈩 鍑虹幇浜嗕竴涓皬鐨勫惛鐑嘲銆?216鈩 鍑虹幇浜嗕竴涓ぇ鐨勫惛鐑嘲銆備粠鐑噸鍙 DSC 鏇茬嚎涓婅兘澶熺湅鍑猴紝鍚勭粍鍒嗕箣闂村苟娌℃湁鐩镐簰浣滅敤锛屾瘡涓潗鏂欓兘浣撶幇浜嗗悇鑷殑杞彉鍜屽垎瑙ｆ晥搴斻€傚彧鏈夊綋娓╁害楂樹簬 1260鈩 鏃讹紝鎵€瑙傚療鍒扮殑鍒嗚В鍙兘鍙犲姞浜嗗叾浠栨潗鏂欑殑鐔旇瀺銆係TA 涓 FT-IR 鐩哥粨鍚堟湁鍔╀簬姝ょ被澶嶆潅鏇茬嚎鐨勮В閲娿€侟/p>

STA-FT-IR瀹為獙锛屾牱鍝佽川閲忥細23.6mg锛孭t/Rh鍧╁煔锛屽崌娓╅€熺巼锛?0k/min锛屾爱姘旀皵姘涳紱
涓婂浘涓紝钃濊壊瀹炵嚎涓 TG 鏇茬嚎锛岃摑鑹茶櫄绾夸负 DTG 鏇茬嚎锛岀孩鑹叉洸绾夸负 DSC 鏇茬嚎銆侟/p>

缁撳悎 FT-IR 鏁版嵁涔嬪悗鍙互鐪嬪嚭锛屽湪 500鈩 浠ュ唴锛屽彧鏈夋按钂告皵閫稿嚭銆傝繖鏄吀鍨嬬殑鐭宠啅浜屾按鍖栧悎鐗╃殑澶辨按杩囩▼锛屽厛鐢变簩姘村悎鐗╁彉鎴愬崐姘村悎鐗╁啀鍙樻垚鏃犳按纭吀閽欍€傜浜屼釜杈冨ぇ鐨勫垎瑙ｆ楠わ紙DTG鐨勫嘲鍊兼俯搴﹀湪 453鈩冿級鏄敱 Ca(OH)2 鐨勮劚姘村紩璧枫€傚湪 362鈩 鏃 DSC 鏇茬嚎涓婄殑灏忔斁鐑嘲鏄敱浜庢棤姘寸～閰搁挋杞彉涓何?纭吀閽欍€傚湪 576鈩 鏃 DSC 鏇茬嚎涓婄殑鍚哥儹宄板垯鏄敱浜庣煶鑻辩敱伪鐩歌嚦尾鐩哥殑鐩歌浆鍙樸€侟/p>

鍦 780鈩 闄勮繎锛孋aCO3 鍒嗚В浜х敓CO2 銆傚湪 1216鈩 鍑虹幇纭吀閽櫸茬浉鑷澄辩浉鐨勭浉杞彉锛岄殢鍚庣～閰搁挋渚垮紑濮嬪垎瑙ｃ€侟/p>

STA-FT-IR 瀹為獙锛孴GA 鏇茬嚎锛堣摑鑹诧級锛孌TG 鏇茬嚎锛堣摑铏氱嚎锛夛紝浜屾哀鍖栫⒊锛堥粦鑹诧級锛屾按锛堥潚鑹诧級锛屼簩姘у寲纭紙绾㈣壊锛堻/p>

Perseus STA-FTIR - 鐩稿叧闄勪欢

PulseTA^?

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